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Presentation
Presentation
The instrumental methods of analysis course aims to enable students to acquire knowledge and skills, such as qualify professionals in the area of instrumental analysis, providing them with a learning that allows become competitive in the labor market
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Class from course
Class from course
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Degree | Semesters | ECTS
Degree | Semesters | ECTS
Bachelor | Semestral | 5
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Year | Nature | Language
Year | Nature | Language
2 | Mandatory | Português
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Code
Code
ULHT2710-3570
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Prerequisites and corequisites
Prerequisites and corequisites
Not applicable
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Professional Internship
Professional Internship
Não
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Syllabus
Syllabus
Theoretical 1-Introduction to Instrumental Methods of Analysis: Concepts and Methodologies in Instrumental Analysis 2. Spectroscopic Methods 2.1. Spectrophotometry / UV / Vis Spectroscopy 2.2. Infrared Spectrophotometry / Spectroscopy 2.3. Spectrophotometry / Atomic Absorption Spectroscopy 2.4. Spectrophotometry / Flame Emission Spectroscopy 2.5 Basic concepts of validation of analytical methods. 3. Separative Techniques 3.1. Gas Phase Chromatography (GC) 3.2. High efficiency liquid chromatography (HPLC) 3.3. Electrophoresis 3.4- Hyphenated Techniques 4. Electroanalytical methods 5. Nuclear magnetic resonance (NMR-1-H, NMR-13C) Practice PL1 - Determination of iron in water PL2-Determination of Acetylsalicylic Acid or Paracetamol in tablets PL3- Determination of Ca by atomic absorption PL4 - Determination of vinegar acidity PL5-Extraction of caffeine in samples PL6-Determination of caffeine in soft drinks by HPLC
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Objectives
Objectives
Acquire knowledge of the principles, instrumentation and applications of the most common analytical techniques, including atomic and molecular absorption spectroscopy, electrochemical and separative methods (chromatographic and electrophoretic); Acquire knowledge about the main extraction and handling processes of solid, liquid and gaseous samples; Know how to implement, develop and validate a method of analysis; Acquire laboratory practice in the use of equipment and know the operating principles, rules and safety conditions of each equipment; Develop communication skills and work in groups; Develop critical thinking.
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Teaching methodologies
Teaching methodologies
Study visits to learn about equipment such as Nuclear Magnetic Resonance, X-rays. Implementation of distance classes for extra student support with additional exercises for homework and better understanding of the subject.
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References
References
D. Harris (2015). Quantitative Chemical Analysis, 8ª edição, Macmillan Learning. D.A. Skoog, D. West, F.J. Holler, S.R. Crounch (2017). Principles of Instrumental Analysis, 7th edition, Brooks Cole.
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Assessment
Assessment
Descrição
Data limite
Ponderação
1ª frequência
2ª frequência/Frequência Global
50%
Relatórios escritos em ppt
Ao longo do semestre
20%
Apresentação e discussão oral
25%
Desempenho Laboratorial Ao longo do semestre 5%
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Mobility
Mobility
No
